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1HPLCELSD法分析注射用硫普罗宁含量及有关物质A1A0A3A2A4A5A6A7A8A9A10A11A12A13A14A15A16A17A18A19A20A21A22A23A24A25A26A27A28A29A30A31A8A32A33A34A35HPLCELSDA36A32A33A37A38A39A40A41A42A43A9KROMASILC18A35250MMA4446MMA455A46MA36A25A26A47A48A47A4930A50A48A51A52A2705A53A54A55A23A3520A4280A36A56A57A58A24A48A57A5908MLA60MIN1A48A28A29A30A31A8A32A33A34A61A62A63A49A6444A50A45A65A6624BARA45A67A68A34A69A39A70A71A70A71A42A72A73A15A74524A46GA752555A46GA76A77A78A79A80A81A82A83A84A85A86A87A88A89A90A18A91A35R09994A36A45A92A93A90A94A95RSDA56108A45A32A33A96A97A98A15A96A99A100A5602A46GA9705A46GA39A70A101A42A37A38A102A59A103A104A105A45A106A107A108A109A110A111A45A92A93A90A88A39A112A113A114A115A114A115A116A7A8A9A10A11A12A13A48A14A15A48A17A18A19A20A48A21A22A23A24A25A26A38A48A28A29A30A31A8A32A33A34A117A118A119A120A121A119A120A122A123A123A124A125A126A124A125A126A127A128A129A130A131A127A128A129A130A122A132HPLCELSDANALYSISOFTIOPRONINFORINJECTIONANDITSRELATEDSUBSTANCESABSTRACTOBJECTIVETODEVELOPANHPLCELSDMETHODFORTHEDETERMINATIONOFTIOPRONINFORINJECTIONANDITSRELATEDSUBSTANCESMETHODMETHODSTHECOLUMNKROMASILC18250MM46MM,5MTHECOLUMNTEMPERATURE30A133THEMOBILEPHASEMETHANOL05ACETICACID2080FLOWRATE08MLA134MIN1THEDRIFTTUBETEMPERATURE44A133GASOPERATIONPRESSURE24BARIMPACTORONRESULTSTHECALIBRATIONCURVEWASLINEARINTHERANGOF524G2555GR09994THEREPEATABILITYRSDWAS108THELIMITOFDETECTIONANDQUANTIFICATIONWERE02GAND05GRESPECTIVELYCONCLUSIONTHEMETHODISSIMPLEANDRAPID,THERESULTSAREACCURATEANDREPRODUCIBLEKEYWORDSTIOPRONINFORINJECTIONCONTENTDETERMINATIONRELATEDSUBSTANCESHPLCELSDA135A136A137A138A139TIOPRONINA140A141A142A143A144N2A145A146A147A148A146A149A150A151A141A152A153A154A155A156A157A158A141A159A160A161A162A163A162A164A165A166A167A168A169A170A171A172A173A174A175A176A177A178A179A180A181A182A183A184A185A186A187A188A189A190A183A191A192A193A194A195A196A197A180A198A199A200A201A202A203A204A205A169A206A207A170A208A209A210A211A212A213A214A201A215A216A217A218A219A220A221A185A186A182A183A222A223A187A189A190A183A191A192A193A194A224A225A226A2271A228A229A230A231A232A233A234A235A236A237A238A239A230A240A241A242A243A244A245A246A247A248A249A250A251A252A253A247A231A232A254A233A234A235A236A237A238A239A255A2A0A230A240A241A242HPLCELSDA30A1A3A4A247A172A3A4A134A5A6A7A8A9A10A11A12A13A14A15A16A17A175A18A19A35A20A21A22A17HPLCUVA35A23A14A9A10A11A12A24A25A26A27A28A29A31A39A184A92A32A93A94A33A39A96A34A16A36A93A100A37A39A83A38A40A41A39A13A159A42A43A44A45A46A47A47A48A49A50A51A52A48A49A50A51A48AGILENT1100A189A53A54A55A56A57A58ALLTECHELSD2000A59A60A61A62A63A64A65A66A58A191A67A68A69N2010A55A56A70A71A72A58KROMASILC18A73250MMA7446MMA755A76MA77A55A56A78A79A80A63A81A82A84A85A86A73A196A87A88A89A143A90A91A95A97A98A99A101A102A103A104A105A106A107A108A109A110A111A112A113A114A115A116A143A117A90A98A99A101A102A103A104A202A118A119A12040A112A206A121A122A209A123A124A117A90A98A99A101A102A103A104A125A126A127A212A128A129A130A131A132A133A135A136A137A137A138A139A140A141A138A139A140A141A1381A142A144A145A146A142A144A147A148KROMASILC18A149250MMA15046MMA1515A152MA153A154A155A156A157A148A158A160A14805A161A162A163A164A14920A14880A153A154A155A165A14808MLA166MIN1A154A147A167A14830A168A154A169A170A171A14810A152LA154A173A174A176A177A178A179A180A181A182A183A185A186A18744A188A190A192A19324BARA190A194A195A181A197A1982A199A200A201A203A204A216A205A207A217A208A178A210A211A213A214A215A218A219A220A221A222A223A224A225A226A227A228A225A229A230A231A225A232A233A234A228A235A236A237A238A239A240A241A234A225A242A228A243A225A231A228A243A22580A244A245A246A247A248A249A250A235A251A252A253A254A255A238A228A247A248A252A0A1A2A243A235A181A3A4A238A239A240A247A248A249A250A86A5A2A6A42A234A7A8A9A10A11A225A202A12A13A1440A235A90A15A253A254A255A238A2A243A235A181A3A4A16A17A18A19A20A2A6A36A21A33A33A40A22A23A24A40A22A23A24A40A2531A43A26A27A43A26A238A28A29A30A31A32A34A35A37A38A39A41A44A45A46A47A48A49A50A51A96A52A53A54A551A66A2437A5632A57A58A59A60A57A58A59A60A244A61A62A63A64A65A67A68A69A70A71A229A72A73A74A75A76A77A78A71A79A80A81A82A83A84A850524GA87L1A930822GA87L1A931079GA87L1A931286GA87L1A931561GA87L1A932016GA87L1A932555GA87L1A88A89A91A92A94A95A97A98A99A100A101A102A103A104A105A106A107A108A109A110A98A250A111A102A103A112A98A113A107A114A115A116MA117A118A114A119A120A121A122A123A116AA117A88A124A125A126A127A107A108A128A129A130A131A132A133,A130A131A134A135LNA14381LNM98287A98A136A137A138A127R09994A98A116N7A117A139A99524A140GA1412555A140GA142A143A144A98A128A129A137A138A145A146A139233A147A148A149A148A149A79A15001MG/MLA9310MG/MLA93100MG/MLA88A114A119A95A97A98A99A100A101A102A103A104A105A106A11310A140LA239A151A152A107A1146A153A98A109A110A121A122A123A98RSDA83A84A85145A93046A93019A13934A154A155A156A155A156A157A158A159A160A161A162A163A164A217A165A166A167A168A169A1706A171A172A173A174A175A176A177A178A179A180A182A183A184A185A186A187A176RSDA188108A18935A190A191A192A191A192A193A194A195A196A197A1988MGA19910MGA19912MGA200A201A203A204A205A206A207A208A209A210A211A212A213A214A215A21640A218A219A220A222A221A223A2243A225A218A226A227A212A230A231A211A232A233A235A236A237A218A254A240A241A242A245A246A247A218A248A24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5A216A217A218A219A220A193A223A224A225A226A227A225A228A230A232A233A234A230A235A236A237A238A239A240A241A242A243A2443参考文献1WS1X0012005Z,TIOPRONINFORINJECTIONA245A246A248A249A250A251A253S2ZHOUZM,HELYDETERMINATIONOFTHEDISSOLUTIONOFTIOPRONINTABLETBYHPLCJPRACTICALPHARMACYANDCLINICALREMEDIESA254A248A255A8A0A1A2,2007,VOL10,NO31901913WANGLP,LIUHL,WUQDETERMINATIONOFTIOPRONININJECTIONBYHPLCJDRUGSTANDARDSOFCHINAA14A3A255A4A5A6,2008,VOL9,NO171734CHP2005VOLA20A21A14A3A255A7A23A9A9A10A26A11A28A29A12A31A13A15A16A28A23A9A9A10A17A36A18A18A19A22A24A25A27A43A30A451A32A33A34A35A37A38A39TAB1THERESULTSOFRECOVERYA40A41A42A44A46A47A48A44A49A50A51A52A44A47A53A42A41A44A54A46A47A48A44A49A50A51A55A44A56A57A46A44A41A58A49A59A40A60A44A47A46A44A41A47A51A44A41A44A56A57A46A44A41A58A49A59A55A61A62A49A59A63A64A65A66A67A64A68A69A68A70A71A64A68A72A67A64A68A71A67A64A69A68A68A70A71A64A69A72A67A64A68A72A67A64A69A69A68A70A71A64A69A69A68A70A64A68A65A68A70A64A69A67A68A70A68A64A67A66A68A70A64A69A73A68A70A64A72A67A68A70A68A64A71A66A68A70A68A64A66A69A70A64A67A65A68A70A64A68A73A68A70A64A72A72A68A70A71A64A67A66A68A68A64A65A66A68A68A64A65A63A68A70A70A64A70A67A68A71A64A72A71A68A71A64A73A72A68A70A70A64A65A63A68A71A64A66A63A68A71A64A63A63A68A70A70A64A63A65A74A75A76A77A7876543210A79A80A81A82100959085807570656055504540353025201510A83A84A85A866475A679334A871A88A89A90A91FIG1TIOPRONINA92A93A94A95A96109876543210A97A98A99A1004442403836343230282624222018161412A101A102A103A104402024A226871A101A102A103A10422598A5724A872A105A106A107A10840FIG2DEXTRAN40876543210A109A110A111A1121251201151101051009590858075706560555045403530252015A113A114A115A116401968AA117A118A119A
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